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Working guidanceWe run this. It has produced results under the conditions stated on this page. · Reviewed 29 August 2026 · The full position record

The Reliable Mash: The Production Mash

Our working baseline for a 100% sorghum malt enzyme mash: hot liquefaction, staged enzyme additions, controlled cooling into conversion range, mash-out, iodine interpretation, and batch records.
Proven in production — an independent lab measured this beer clean

We ran this baseline at commercial scale to make Bard’s Gold, a 100% sorghum-malt gluten-free beer: ~90% apparent attenuation, 4.87% ABV, 3.1 SRM, sound pH, microbiologically clean, diacetyl below threshold. The full panel and what it does not prove are below.

Watch on YouTubeHow a 100% Sorghum Mash Actually RunsThe protocol end to end, and the reasoning behind each step. AI-generated from this page and reviewed for accuracy.7:04

The run sheet​

The run sheet carries every target, addition, and stop condition. The thermal profile further down is the shape those steps produce: liquefy hot, cool into the conversion band, stage each enzyme, mash out, then run off to an iodine-negative endpoint.

Stir continuously. Most of what goes wrong in this mash traces back to settling, uneven heat, or poor enzyme contact.

Brew-Day Run Sheet

100% Sorghum Malt Enzyme Mash

Protocol
GFB-RELIABLE
Version
Public 1.2
Effective
August 2026

Working baseline for 100% sorghum malt. Do not reuse this sequence for millet, rice, corn, or mixed-grist mashes.

Critical: Use the full 190°F (88°C), 60-minute liquefaction baseline; stage each enzyme at the specified temperature; stir continuously; record every change.

Initial water2.2–3.0 L/kg (about 1.0–1.4 qt/lb)Production ran both ends of this range; calculate cooling water separately
Mash pH5.5–5.6Measure and record actual pH
CalciumApproximately 100 ppmComplete-process working baseline
MixingContinuousRequired through every mash hold

Stage before grain-in

Format
1
Liquefy

Mash in and open the starch

190°F (88°C)60 minutes
Do
Bring the full liquor to temperature with the initial Termamyl dose already in the water, agitator at full speed. Then add the sorghum malt slowly — never dumped — so liquefaction keeps pace with gelatinization, and stir continuously through the hold. Rice hulls do NOT go in here; they are added at mash-out for the transfer.
Add
  • 100% sorghum malt, added slowly into enzyme-active hot liquor
  • Termamyl SC DS: 1 mL/lb sorghum malt — in the water before any grain
Advance when
The full hold is complete and the mash remains evenly heated, mixed, and pumpable.
Record
Actual temperature path · Hold time in range · Mixing behavior · Enzyme product, dose, and lot
More detail for step 1
2
Convert

Cool and begin lower-temperature enzyme work

145°F (63°C)45 minutes
Do
Cool or dilute according to the pre-calculated plan. Add Ondea Pro and the second Termamyl dose, then continue stirring.
Add
  • Ondea Pro: 1.5 mL/lb sorghum malt
  • Termamyl SC DS: 0.75 mL/lb sorghum malt
  • Calculated cooling or dilution water
Advance when
The mash has completed 45 minutes at the target conversion temperature.
Record
Cooling water added · Final mash thickness · Actual pH · Time at target temperature
More detail for step 2
3
Finish

Finish the fermentability work

145°F (63°C)10 minutes
Do
Keep the mash at conversion temperature, add Amylase AG 300L, and continue mixing through the finishing hold.
Add
  • Amylase AG 300L: 0.75 mL/lb sorghum malt
Advance when
The 10-minute finishing-enzyme hold is complete.
Record
Addition time · Enzyme product, dose, and lot · Temperature · Hold time
More detail for step 3
4
Mash out

Raise the mash for wort separation

180°F (82°C)10 minutes
Do
Raise the mash to 180°F (82°C) while continuing to mix; the glucoamylase can survive lower mash-out temperatures through a slow lauter and quietly over-attenuate the wort. Add the rice hulls now and mix 5–10 minutes before transfer — they are runoff structure, not a mash ingredient, and they do their job in the lauter bed. Do not shorten the scheduled conversion or finishing holds.
Add
  • Rice hulls: begin around 5% of malt weight when bed behavior is uncertain; mix 5–10 minutes before transfer
Advance when
The 10-minute mash-out hold is complete and the mash is ready for separation.
Record
Ramp start and finish · Time at mash-out · Mixing behavior · Any approved deviation
More detail for step 4
5
Separate

Run off, verify the endpoint, and transfer

Final wortIodine negative
Do
Record the iodine sample point, separate the wort, track runoff and clarity, and transfer the wort to the kettle.
Add
None
Advance when
Final wort is iodine negative, kettle transfer is complete, and the batch record is filled in.
Record
Sample point, time, and temperature · Mash or wort sample · Runoff behavior · Wort clarity and gravity
More detail for step 5
StepActionTargetAddAdvance when
1. Liquefy: more detailBring the full liquor to temperature with the initial Termamyl dose already in the water, agitator at full speed. Then add the sorghum malt slowly — never dumped — so liquefaction keeps pace with gelatinization, and stir continuously through the hold. Rice hulls do NOT go in here; they are added at mash-out for the transfer.190°F (88°C)
60 minutes
  • 100% sorghum malt, added slowly into enzyme-active hot liquor
  • Termamyl SC DS: 1 mL/lb sorghum malt — in the water before any grain
The full hold is complete and the mash remains evenly heated, mixed, and pumpable.
2. Convert: more detailCool or dilute according to the pre-calculated plan. Add Ondea Pro and the second Termamyl dose, then continue stirring.145°F (63°C)
45 minutes
  • Ondea Pro: 1.5 mL/lb sorghum malt
  • Termamyl SC DS: 0.75 mL/lb sorghum malt
  • Calculated cooling or dilution water
The mash has completed 45 minutes at the target conversion temperature.
3. Finish: more detailKeep the mash at conversion temperature, add Amylase AG 300L, and continue mixing through the finishing hold.145°F (63°C)
10 minutes
  • Amylase AG 300L: 0.75 mL/lb sorghum malt
The 10-minute finishing-enzyme hold is complete.
4. Mash out: more detailRaise the mash to 180°F (82°C) while continuing to mix; the glucoamylase can survive lower mash-out temperatures through a slow lauter and quietly over-attenuate the wort. Add the rice hulls now and mix 5–10 minutes before transfer — they are runoff structure, not a mash ingredient, and they do their job in the lauter bed. Do not shorten the scheduled conversion or finishing holds.180°F (82°C)
10 minutes
  • Rice hulls: begin around 5% of malt weight when bed behavior is uncertain; mix 5–10 minutes before transfer
The 10-minute mash-out hold is complete and the mash is ready for separation.
5. Separate: more detailRecord the iodine sample point, separate the wort, track runoff and clarity, and transfer the wort to the kettle.Final wort
Iodine negative
NoneFinal wort is iodine negative, kettle transfer is complete, and the batch record is filled in.
Authority, limitations, and review control

This is one selected GFB working protocol developed from Bard's commercial gluten-free brewing experience and direct technical collaboration with Novozymes. Its values are practical working targets, not universal manufacturer instructions. Pilot the actual malt, water, enzymes, and equipment before production use.

Review when: an enzyme product changes, material or equipment changes, contradictory production evidence appears, or the calcium rationale is resolved.

Read the evidence behind the 190°F baseline

Level 2 · Detailed Procedure

Run each step with its checks and context

Use the run sheet during a routine mash. Use these expanded steps when setting up the process, training an operator, documenting a deviation, or diagnosing unexpected behavior.

Mash in and open the starch

Objective

Hydrate the sorghum, expose its starch, and make the mash evenly mixed and pumpable before lower-temperature conversion begins.

Operating instruction

Bring the full liquor to temperature with the initial Termamyl dose already in the water, agitator at full speed. Then add the sorghum malt slowly — never dumped — so liquefaction keeps pace with gelatinization, and stir continuously through the hold. Rice hulls do NOT go in here; they are added at mash-out for the transfer.

Add
  • 100% sorghum malt, added slowly into enzyme-active hot liquor
  • Termamyl SC DS: 1 mL/lb sorghum malt — in the water before any grain

What good looks like

The full hold is complete and the mash remains evenly heated, mixed, and pumpable.

Watch for

Clumping, settling, uneven heating, rising mixer load, or a mash that does not become workable.

If this happens

Confirm temperature distribution, the initial Termamyl addition, and continuous mixing before changing rice-hull or enzyme dose.

Record

Actual temperature path · Hold time in range · Mixing behavior · Enzyme product, dose, and lot

Level 3 · Mechanism and evidence Why the 190°F baseline exists

Cool and begin lower-temperature enzyme work

Objective

Move the liquefied mash into the operating range for conversion and fermentability work without losing control of mash thickness or the batch record.

Operating instruction

Cool or dilute according to the pre-calculated plan. Add Ondea Pro and the second Termamyl dose, then continue stirring.

Add
  • Ondea Pro: 1.5 mL/lb sorghum malt
  • Termamyl SC DS: 0.75 mL/lb sorghum malt
  • Calculated cooling or dilution water

What good looks like

The mash has completed 45 minutes at the target conversion temperature.

Watch for

Overshooting the cooling target, incomplete mixing, or unrecorded dilution that makes later batches impossible to compare.

If this happens

Pause additions until the actual temperature and water addition are known. Correct the record first; do not guess the final mash thickness.

Record

Cooling water added · Final mash thickness · Actual pH · Time at target temperature

Level 3 · Mechanism and evidence External enzyme strategy

Finish the fermentability work

Objective

Give the finishing enzyme its scheduled contact time so the wort profile is built before mash-out stops the intended lower-temperature work.

Operating instruction

Keep the mash at conversion temperature, add Amylase AG 300L, and continue mixing through the finishing hold.

Add
  • Amylase AG 300L: 0.75 mL/lb sorghum malt

What good looks like

The 10-minute finishing-enzyme hold is complete.

Watch for

Raising to mash-out before the scheduled finishing hold is complete.

If this happens

Hold at 145°F (63°C) until the scheduled finishing contact time is complete. Record any early temperature movement as a protocol deviation.

Record

Addition time · Enzyme product, dose, and lot · Temperature · Hold time

Level 3 · Mechanism and evidence Enzyme conversion in the mash

Raise the mash for wort separation

Objective

End the intended enzyme work — including the glucoamylase, which is harder to stop than spec sheets suggest — then prepare the mash for controlled wort separation.

Operating instruction

Raise the mash to 180°F (82°C) while continuing to mix; the glucoamylase can survive lower mash-out temperatures through a slow lauter and quietly over-attenuate the wort. Add the rice hulls now and mix 5–10 minutes before transfer — they are runoff structure, not a mash ingredient, and they do their job in the lauter bed. Do not shorten the scheduled conversion or finishing holds.

Add
  • Rice hulls: begin around 5% of malt weight when bed behavior is uncertain; mix 5–10 minutes before transfer

What good looks like

The 10-minute mash-out hold is complete and the mash is ready for separation.

Watch for

An early temperature rise that cuts off intended enzyme-contact time.

If this happens

Verify that both 145°F (63°C) holds were completed before continuing. If they were shortened, record the deviation rather than silently extending another stage.

Record

Ramp start and finish · Time at mash-out · Mixing behavior · Any approved deviation

Level 3 · Mechanism and evidence Temperature programs

Run off, verify the endpoint, and transfer

Objective

Recover usable wort, distinguish conversion from separation behavior, and finish with an interpretable iodine result and complete batch record.

Operating instruction

Record the iodine sample point, separate the wort, track runoff and clarity, and transfer the wort to the kettle.

What good looks like

Final wort is iodine negative, kettle transfer is complete, and the batch record is filled in.

Watch for

Treating an intermediate positive iodine check as the final result or changing enzyme dose before locating the real bottleneck.

If this happens

Identify the sample point and confirm whether the problem is conversion, retained wort, compaction, or solids carryover before changing the next batch.

Record

Sample point, time, and temperature · Mash or wort sample · Runoff behavior · Wort clarity and gravity

Level 3 · Mechanism and evidence Sorghum mash challenges

Watch on YouTubeThe Reliable Mash, Step by StepThe protocol as a run sheet — every step, in order, in ninety seconds. AI-generated from this page and reviewed for accuracy.1:38
How the three relate

The Cereal Decoction was the first approach tried. The Maltose Mash is the design that ran as Bard's original production mash, and whose chemistry — through toll-processed extract — made most of the beer Bard's ever sold. The Reliable Mash is the redesign that replaced it on the brewhouse floor, and the one whose brewhouse records we hold.

Worth knowing before you run this: this is the one with the records — production data, an independent lab panel and four years of batch QA — which is what lets us help you diagnose a batch that goes sideways. It is not the beer Craig would brew. He would brew the Maltose Mash, and says so in his own words there. Run this one if you want the process we can support you on; run that one if you want the beer we would rather drink and will write down what happened. The two, side by side.

These used to be numbered Mash Protocol 1, 2 and 3. The numbers were retired on 2026-08-30 because they implied a sequence that was not merely uninformative but backwards: the numbering ran 1, 2, 3 while the history ran Cereal Decoction, Maltose Mash, Reliable Mash.

The February 2019 lab panel, and what it does not establish

This is not a theoretical recipe. We ran it at commercial scale to make Bard's Gold, a 100% sorghum-malt gluten-free beer that an independent lab measured as:

MeasureResultWhat it shows
Apparent attenuation~90%The staged external-enzyme mash built a highly fermentable wort — fully converted, dry, clean
Alcohol by volume4.87%On style for a sessionable gluten-free lager
Color3.1 SRMBright pale gold
pH~4.0Sound finished-beer pH
Wild yeast, aerobic + anaerobic bacteriaall negativeMicrobiologically clean
Diacetylbelow thresholdWell-managed fermentation

That confirms the beer is real and clean. It does not by itself establish the gluten-free claim — that rests on the pre-fermentation evidence in the QA Trust Chain.

The figures above are from an independent brewing QC laboratory panel on the finished flagship, February 2019. That panel itself is not published — it sits in the source archive, and this table is what it recorded. What is published, and checkable, is the surrounding production evidence: the Production QA Log 2014–2017 carries 155 stage-by-stage batch records including the per-batch gliadin-negative results, the LCBO finished-beer certificates are a regulator's own numbers on the same beer, and Fermentation Management sets the February 2019 figures against four years of RDF data.

On the 60-minute liquefaction hold

A 30-minute hold at 190°F (88°C) worked in most of our runs. The 60 minutes specified below is production insurance against malt-lot, equipment, heating, mixing, and scale variability — not the minimum time conversion requires. A 100-minute hold is the belt-and-braces option where a failed batch is not survivable. All three rungs, and how to choose, are on the liquefaction ladder. Validate a shorter hold on your own malt and equipment across several batches before you adopt it. See why the 190°F baseline exists.

Where the source documents disagree with each other

Four production documents describe this mash. They agree on nearly everything, and where they don't, we say so rather than pick a winner quietly.

The 145°F conversion step. Three of the four give 45 minutes. One — plausibly an earlier or parallel working draft — gives 35. The run sheet carries 45 because that's the better-supported value; the 35-minute document exists and disagrees, and a reader validating this on their own system should know that.

The water-to-malt ratio. The documents carry 1.0, 1.2 and 1.4 qt/lb between them, attributed to different sources and calculation paths within the same spreadsheet. That is why the sheet states a range rather than one figure: production ran both ends of it.

Neither disagreement touches the protected baseline — the 190°F, 60-minute liquefaction is unanimous across every source found.

If you've brewed barley, this temperature is where your instincts object

A barley mash lives around 148–162°F (64–72°C) because conversion depends on the malt's own enzymes, and heat like this would end them. That instinct is correct for barley. Here it's exactly backwards. In the GFB method, conversion does not depend on the malt's enzymes at all: external enzymes own it, and the liquefaction enzyme added at this step is chosen to work at this heat. Sorghum starch also gelatinizes hotter than barley starch, so the mash needs this temperature to open the starch in the first place. The 190°F (88°C) hold is not a hazard to survive. It is the reason the rest of the protocol works.

The Reliable Mash temperature-vs-time profileA line showing mash temperature over time for the 100% sorghum-malt enzyme mash: a 60-minute hold at 190°F to liquefy, a cool-down to a 55-minute conversion band at 145°F, a rise to a 10-minute mash-out at 180°F, then runoff to an iodine-negative endpoint. Termamyl is added at mash-in, Ondea Pro and Termamyl at the start of the 145°F band, and Amylase AG 300L 45 minutes in.145°F63°C180°F82°C190°F88°Crunoff → iodine negativeTermamyl SC DS · 2 mL/lbOndea Pro 1.5 + Termamyl 0.75Amylase AG 300L · 0.75Liquefy60 min · 190°FConvert45 min · 145°FFinish10 min · 145°FMash out10 min · 180°F
mash temperature enzyme additionHold widths are drawn to their minutes; the cool-down and heat-up ramps are schematic, not timed baselines. This mirrors the GFB-RELIABLE run sheet above — use the run sheet for the controlling values, targets, and stop conditions.

Scale this protocol to your batch​

Enter your sorghum-malt weight to scale the documented per-pound additions. This is a planning aid for the working baseline above — validate the result on your own malt and equipment.

lb
AdditionWhenBasisYour batch
Initial waterMash-in≈ 1.4 qt/lb140 qt35 gal
Rice hullsMash-out (when bed behavior is uncertain)≈ 5% of malt weight5 lb
Termamyl SC DS190°F (88°C) — liquefaction, at mash-in1 mL/lb (V12 sheet; corrected from the pilot's 2 mL/lb on 2026-09-07)100 mL
Ondea Pro145°F (63°C) — conversion1.5 mL/lb150 mL
Termamyl SC DS (2nd dose)145°F (63°C) — conversion0.75 mL/lb75 mL
Amylase AG 300L145°F (63°C) — finishing0.75 mL/lb75 mL

Scales the documented per-pound basis of The Reliable Mash to your grain bill. It is a starting point to validate on your own malt, water, and equipment — not a universal recommendation. Cooling/dilution water is calculated separately (add only what reaches 145°F), and pH 5.5–5.6 and ≈ 100 ppm calcium are targets set against your source water, not quantities that scale with grain weight. Record the actual product, dose, and lot for every addition.

After the run​

Continue to the boil

The batch reached its operating endpoint.

  • Final wort is iodine negative.
  • Runoff behavior is normal for the equipment and grist.
  • Target gravity is reached.
  • The batch record is complete.
Pause and investigate

Do not change the next batch from a guess.

For stuck or slow runoff, weak conversion, or unusual mash behavior, identify the bottleneck in Sorghum Mash Challenges before changing enzyme dose or temperature.

Interpret the iodine result​

Don't treat an intermediate positive mash iodine check as the final result. Starch-degrading enzymes may continue working during wort separation; final wort should be iodine negative.

Record the sample point, time, temperature, result, and whether the sample was mash or wort.

Complete the batch record​

Identity and materials
  • GFB-RELIABLE, public version 1.2, and any approved deviation
  • Sorghum malt lot and crush profile
  • Enzyme product, dose, lot, and addition time
  • Source water and mineral, acid, chloride, and sulfate additions
Actual process
  • Initial and cooling water, final mash thickness, and rice-hull use
  • Actual pH, temperature path, and hold times
  • Stirring, settling, clumping, mixer load, and other handling observations
Wort and separation
  • Iodine sample point and result
  • Gravity, runoff behavior, and wort clarity or turbidity
Downstream result
  • Fermentation performance, attenuation, and final gravity
  • Finished-beer body, dryness, mouthfeel, balance, and sensory notes

→ Print or download the blank batch record — a print-ready sheet for the brewhouse (also saves as PDF).

See Batch Records for the complete recording system.

Technical basis and open questions​

Technical basisThe 190°F (88°C), 60-minute hold is our conservative production baseline for repeatability.

We ran this hold at Bard's across changing malt lots, equipment, and production conditions, and it was highly reliable in the runs our records preserve. We keep it as a deliberately conservative baseline — not because it's mandatory, and not because we have proven it optimal.

Open research questionLower temperatures or shorter holds may work, but the reliable boundary has not been established.

The open question is how far the temperature, the hold time, or both can be reduced without sacrificing liquefaction, mash handling, extract, runoff, fermentation performance, finished-beer quality, or repeatability across malt lots and equipment. A useful study compares controlled alternatives across multiple batches and malt lots rather than treating one successful batch as proof.

Reference valuesWorking dosing and process basis
ItemProtocol valueNotes
Sorghum malt basis100% sorghum maltDose enzymes per lb of sorghum malt.
Water-to-malt ratio2.2–3.0 L/kg (about 1.0–1.4 qt/lb) initial, with cooling/dilution water recorded separatelyProduction ran both ends of this range. State the units whenever you write a ratio down — L/kg and qt/lb differ by ~2×, and an unlabeled ratio reads as a conflict when it is really arithmetic. Record initial water, cooling/dilution water, and final mash thickness after the mash reaches 145°F (63°C).
Cooling/dilution waterCalculated separately before mash-inAdd only what is needed to reach 145°F (63°C); record added water and final mash thickness.
Rice hull basisBegin around 5% of sorghum malt weight when bed behavior is uncertain, then reduce where experience shows less is sufficient — added at mash-out, mixed 5–10 minutes before transferHulls are runoff structure, not a mash ingredient: they do their work in the lauter bed, so they go in after conversion, not into the hot liquefaction. Working recommendation, not a fixed requirement. Adjust on bed structure, compaction, runoff, and wort separation. Record actual weight and timing.
Termamyl SC DS initial dose basis1 mL/lb sorghum maltAdd at the beginning of the 190°F (88°C) liquefaction step. Provenance in the next panel.
Ondea Pro dose basis1.5 mL/lb sorghum maltAdd after cooling or dilution to 145°F (63°C).
Additional Termamyl SC DS dose basis0.75 mL/lb sorghum maltAdd with Ondea Pro at 145°F (63°C).
Amylase AG 300L dose basis0.75 mL/lb sorghum maltAdd during the 145°F (63°C) finishing enzyme step. Glucoamylase finish → a glucose-forward wort: very fermentable and reliably dry. For what that means and the maltose-forward alternative, see The Sugar Bible.
pH target5.5 to 5.6Measure and record actual pH by step.
Calcium target / mineral conditionApproximately 100 ppm calciumCurrent complete-process working baseline. Measure source water and record calculated additions and actual profile.
Chloride/sulfate noteRestrained where practical; process-specific, not universalTrack additions. Source water and beer style still matter, and high levels can interfere with enzyme performance.
Stirring requirementContinuous stirring through the mashPrevent settling, uneven heat, poor hydration, and weak enzyme contact.
Reference valuesWhere the Termamyl dose comes from

The 1 mL/lb mash-in dose and the 0.75 mL/lb at coolback are the figures on Bard's last production sheet (Enhanced Protocol V12, July 2020). Every rung below was read from the source named; the doses are stated as each source wrote them, with the per-pound equivalent beside.

SourceDose as writtenPer lb of sorghum malt
Novozymes Brewing Handbook 2013, p. 28 — Termamyl SC DS on a barley-adjunct cereal cooker0.42 lb (0.19 kg) per metric ton of adjunctabout 0.07 mL/lb
Homebrew community table (Zero Tolerance wiki, Termamyl L)0.227–0.363 mL/lb0.23–0.36 mL/lb
Bard's V12 protocol, the column headed "documented"600 mL per metric ton (about 0.27 mL/lb)0.27 mL/lb
Bard's V12 protocol, working sheet (July 2020)1 mL/lb at mash-in + 0.75 mL/lb at coolback1.75 mL/lb total
Bard's 42-barrel production brew, May 20209.5 lb (4.3 kg) of enzyme on 2,300 lb (1,043 kg) of maltabout 1.5 mL/lb total
Bard's pilot protocol v5/v6, November 2019150 mL on 67 lb (30 kg) of malt2.24 mL/lb at mash-in

An earlier version of this page carried the pilot's figure — 2 mL/lb at mash-in — as the production baseline; corrected to the V12 sheet on 2026-09-04. The maker's rate is what the enzyme needs to liquefy a barley-adjunct cereal cook. Sorghum on its own malt was run far above it on purpose, and the reasoning — guaranteed conversion over an optimised enzyme bill — is on the homebrew-scale page. Nobody has published the curve between the maker's rate and ours; that's Research Ask 6.

Reference rationaleApproximately 100 ppm calcium is a complete-process baseline, not a Termamyl minimum.

Novozymes brewing documentation states that Termamyl SC DS can operate at calcium levels below 20 ppm. That is a statement about what the enzyme can tolerate, and it is not the basis for the complete water profile we use here.

Our commercial records at Bard's, along with period distributor guidance on the Novozymes system, ran a higher complete-process calcium condition. We have not recovered the original reason for it. Until we do, target approximately 100 ppm calcium, calculate additions from your source-water profile, and record calcium, chloride, sulfate, acid, and salt additions.

Mechanism and evidence​

Research needed (2)